Hydrofluoric. Burns through silicates and supertoxic, causing tetany and cardiac arrest through fluoride poisoning.
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I was an organic chemist, so mostly working in organic solutions due to low substrate water solubility (esp for fatty t-butyldimethylsilyl deprotections). I used commercially available TBAF in THF. Or if my stuff was acid stable, just stir it with tosic acid or CSA.
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I once read a protocol for using acyl chlorides in aqeuous solution. Took it to an organics prof. He said yeah don't always believe the methodology even if you insist on believing the results :D
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